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Kurajica, S., Popovic, J., Kraljevic, G. T., Tkalcec, E., Simcic, I., Mandic, V., Altomare, A., Moliterni, A. & Rocquefelte, X. (2014) A structural investigation of tris(ethyl acetoacetate)aluminium (III). J. Sol-Gel Sci. Technol. 71 217–223.
Added by: Laurent Cournède (2016-03-10 21:01:55) |
| Type de référence: Article DOI: 10.1007/s10971-014-3345-1 Numéro d'identification (ISBN etc.): 0928-0707 Clé BibTeX: Kurajica2014 Voir tous les détails bibliographiques  |
Catégories: MIOPS Mots-clés: 110 k, aluminum alkoxides, chelating-agents, chemistry, complexes, NMR spectroscopy, phase, Sol-gel, Stability, Structure determination form XRPD, Tris(ethyl acetoacetate) aluminium (III) Créateurs: Altomare, Kraljevic, Kurajica, Mandic, Moliterni, Popovic, Rocquefelte, Simcic, Tkalcec Collection: J. Sol-Gel Sci. Technol. |
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Aluminium tris(ethyl acetoacetate), Al(C6H9O3)(3) has been prepared and characterized by means of H-1 and C-13 nuclear magnetic resonance spectroscopy, scanning electron microscopy and X-ray powder diffraction (XRPD). It was determined that two stereoisomeric complexes can be distinguished in the solution: meridional and facial. The crystal structure of Al(C6H9O3)(3) has been determined from XRPD data. The compound crystallizes in the monoclinic space group P2(1)/n.
Added by: Laurent Cournède |