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Djerdj, I., Cao, M., Rocquefelte, X., Cerny, R., Jaglicic, Z., Arcon, D., Potocnik, A., Gozzo, F. & Niederberger, M. (2009) Structural Characterization of a Nanocrystalline Inorganic-Organic Hybrid with Fiberlike Morphology and One-Dimensional Antiferromagnetic Properties. Chem. Mat. 21 3356–3369. 
Added by: Laurent Cournède (2016-03-10 21:41:23)
Type de référence: Article
DOI: 10.1021/cm901345h
Numéro d'identification (ISBN etc.): 0897-4756
Clé BibTeX: Djerdj2009
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Catégories: MIOPS
Mots-clés: chemistry, electron-spin-resonance, frameworks, metal-oxide nanoparticles, nanorods, nanostructures, networks, nonaqueous synthesis, optoelectronic devices, routes
Créateurs: Arcon, Cao, Cerny, Djerdj, Gozzo, Jaglicic, Niederberger, Potocnik, Rocquefelte
Collection: Chem. Mat.
Consultations : 4/674
Indice de consultation : 2%
Indice de popularité : 0.5%
Résumé     
{A new nanocrystalline inorganic-organic hybrid compound, VO(C6H5COO)(2) has been synthesized under solvothermal conditions by reacting vanadium(V) oxytriisopropoxide with benzoic acid in toluene. A detailed investigation of the composition, structure and properties Of VO(C6H5COO)(2) using chemical and thermal analysis, synchrotron X-ray powder diffraction, electron microscopy techniques including SEM, TEM and SAED, spectroscopy techniques like XPS, EDX and FTIR, SQUID magnetometry and EPR is carefully described. Due to the low-crystallinity of the final material, its crystal structure has been solved from synchrotron X-ray powder diffraction data by combining a direct space global optimization technique and DFT geometry optimization and subsequently refined by the constraint Rietveld method. The compound crystallizes in the monoclinic system with a = 20.652(3)
Added by: Laurent Cournède  
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