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Mansar, A. & Serier-Brault, H. (2022) Microwave-assisted synthesis to prepare metal-organic framework for luminescence thermometry. Journal of Solid State Chemistry, 312 123183. 
Added by: Richard Baschera (2022-07-21 09:05:04)   Last edited by: Richard Baschera (2022-07-21 09:05:48)
Type de référence: Article
DOI: 10.1016/j.jssc.2022.123183
Numéro d'identification (ISBN etc.): 0022-4596
Clé BibTeX: Mansar2022
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Catégories: MIOPS
Créateurs: Mansar, Serier-Brault
Collection: Journal of Solid State Chemistry
Consultations : 6/277
Indice de consultation : 10%
Indice de popularité : 2.5%
Liens URLs     https://www.scienc ... /S0022459622003085
The lanthanide metal-organic framework, La1.23Na0.30(1,3-BDC)2(H2O)·4H2O (1,3-BDC: 1,3-benzenedicarboxylate), has been for the first time synthesized under microwave-assisted hydrothermal conditions with a synthesis duration of 5 min. The substitution of La3+ by Eu3+ and Tb3+ was possible until a maximal content of 10%.mol and the investigation of luminescence properties reveals that emitting cations can be located in the chains formed by the LnO10 polyhedra but also into the polar channels proposed by the structure, where some La3+ crystallographic sites are also available. Finally, when codoped by Eu3+ and Tb3+, the materials exhibit thermometric properties in the cryogenic range with a maximal relative thermal sensitivity around 1% K−1 at 80 K.
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