Sarthou, J., Aballea, P., Patriarche, G., Serier-Brault, H., Suganuma, A., Gredin, P. & Mortier, M. (2016) Wet-Route Synthesis and Characterization of Yb:CaF2 Optical Ceramics. J. Am. Ceram. Soc. 99 1992–2000.
Added by: Richard Baschera (2016-11-03 09:14:54) Last edited by: Richard Baschera (2016-11-03 09:17:28) |
Type de référence: Article DOI: 10.1111/jace.14216 Numéro d'identification (ISBN etc.): 0002-7820 Clé BibTeX: Sarthou2016 Voir tous les détails bibliographiques |
Catégories: MIOPS Mots-clés: crystals, doped caf2 ceramics, fabrication, laser performance, nanoceramics, nd-yag ceramics, segregation, yb Créateurs: Aballea, Gredin, Mortier, Patriarche, Sarthou, Serier-Brault, Suganuma Collection: J. Am. Ceram. Soc. |
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Résumé |
This paper reports a new strainless fabrication method for ytterbium-doped CaF2 laser ceramics involving no drying step before green body casting. The nanoparticles were kept in aqueous solution until green body shaping. Centrifugation was used to obtain correct compactness of the green body before sintering. Characterizations were conducted at different steps of the fabrication process. No grain boundaries oxidation was observed in the sintered ceramics although the nanoparticles were permanently maintained in water until they were sintered. Finally, these ceramics are more homogeneous and have less light scattering defects (no porosity), and present improved optical properties when compared to ceramics obtained from dried nanopowders.
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